(1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

Base Information

Chemical Name:(1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene
CAS No.:1000669-82-8
Molecular Formula:C₃₅H₅₂O₂Si₂
Molecular Weight:560.968
Hs Code.:

Synonyms:(1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

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Chemical Property of (1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

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Technology Process of (1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

There total 2 articles about (1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1000669-80-6
(1R,2R)-1-{(R)-(E)-5-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-hept-1-en-6-ynyl}-2-[tert-butyl-diphenylsilanyloxymethyl]-cyclopropane

: 1000669-79-3
(1R,3aS,6R)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,3a,6,7-hexahydro-azulene

: 1088705-32-1
C₃₅H₅₂O₂Si₂

: 1000669-82-8
(1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

Guidance literature:: [CpRu(CH₃CN)3]+PF₆-; In acetone; at 23 ℃; for 1h;
DOI:10.1021/ja076165q

Reference yield: 15.0%

: C₃₅H₅₂O₂Si₂

: 1000669-79-3
(1R,3aS,6R)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,3a,6,7-hexahydro-azulene

: 1088705-32-1
C₃₅H₅₂O₂Si₂

: 1000669-82-8
(1R,6S)-1-[(R)-1-(tert-butyl-dimethylsilanyloxy)-ethyl]-6-(tert-butyl-diphenyl-silanyloxymethyl)-1,2,3,5,6,7-hexahydro-azulene

Guidance literature:: With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In acetone; at 23 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja806724x