methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside
CAS No.:180580-35-2
Molecular Formula:C₅₅H₆₀O₁₀
Molecular Weight:881.075
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

There total 3 articles about methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 33639-77-9
perbenzyl fucosyl bromide

: 73445-27-9
methyl 3,4,6-tri-O-benzyl-β-D-galactopyranoside

: 180580-35-2
methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; tetraethylammonium bromide; In dichloromethane; for 108h;
DOI:10.1016/0008-6215(96)00030-4

Reference yield:

: 68779-52-2
1,2-O-(1-methoxyethylidene)-3,4,6-tri-O-benzyl-α-D-galactopyranose

: 180580-35-2
methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / mercuric bromide, 2,2,2-trichloroethanol / nitromethane / 16 h / Ambient temperature

2: 70 percent / sodium methoxide / methanol / 24 h

3: 96 percent / tetraethylammonium bromide, molecular sieves 4A / CH₂Cl₂ / 108 h

With 1,1,1-trichloroethanol; 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; mercury dibromide; In methanol; nitromethane; dichloromethane;
DOI:10.1016/0008-6215(96)00030-4

Reference yield:

: 161953-85-1
methyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside

: 180580-35-2
methyl 3,4,6-tri-O-benzyl-2-O-(tri-O-benzyl-α-L-fucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium methoxide / methanol / 24 h

2: 96 percent / tetraethylammonium bromide, molecular sieves 4A / CH₂Cl₂ / 108 h

With 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/0008-6215(96)00030-4