3,4-Dimethoxyphenylmalonaldehydic Acid

Base Information

• Chemical Name: 3,4-Dimethoxyphenylmalonaldehydic Acid
• CAS No.: 77508-31-7
• Molecular Formula: C₁₁H₁₂O₅
• Molecular Weight: 224.213
• Mol file: 77508-31-7.mol

Synonyms:3,4-Dimethoxyphenylmalonaldehydic Acid

Chemical Property of 3,4-Dimethoxyphenylmalonaldehydic Acid

Chemical Property:

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Technology Process of 3,4-Dimethoxyphenylmalonaldehydic Acid

There total 1 articles about 3,4-Dimethoxyphenylmalonaldehydic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

3,4-dimethoxy-trans-cinnamic acid (14737-89-4) → 3,4-Dimethoxyphenylmalonaldehydic Acid (77508-31-7) + 2,6-bis-(3,4-dimethoxyphenyl)-3,7-dioxabicyclo<3.3.0>octane-4,8-dione (69854-19-9)

Guidance literature:

With boron trifluoride diethyl etherate; thallium(III) trifluoroacetate; In dichloromethane; trifluoroacetic acid; for 0.000277778h; Ambient temperature;

DOI:10.1021/jo00328a018

upstream raw materials:

3,4-dimethoxy-trans-cinnamic acid