N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

Base Information

Chemical Name:N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine
CAS No.:1268720-58-6
Molecular Formula:C₂₈H₃₇N₃O₂
Molecular Weight:447.621
Hs Code.:

N<sub>1</sub>-(3,4-dimethoxybenzyl)-N<sub>6</sub>-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

Synonyms:N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

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Chemical Property of N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

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Technology Process of N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

There total 8 articles about N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 249290-16-2
N¹-(1,2,3,4-tetrahydroacridin-9-yl)pentane-1,5-diamine

: 1268720-58-6
N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

Guidance literature:: 3,4-dimethoxy-benzaldehyde; N¹-(1,2,3,4-tetrahydroacridin-9-yl)pentane-1,5-diamine; With diethylamine; In toluene; Reflux;

With palladium on activated charcoal; hydrogen;
DOI:10.1016/j.ejmech.2019.07.053

Reference yield:

: C₂₈H₃₅N₃O₂

: 1268720-58-6
N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 4h;
DOI:10.1016/j.bmc.2010.12.022

Reference yield:

: 96447-10-8
spiro<2H-3,1-benzoxazine-2,1'-cyclohexan>-4(1H)-one

: 1268720-58-6
N₁-(3,4-dimethoxybenzyl)-N₆-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 120 °C

2: potassium iodide / pentan-1-ol / 10 h / 160 °C / Reflux

3: methanol / 4 h / 20 °C

4: sodium tetrahydroborate / methanol / 4 h / 20 °C

With sodium tetrahydroborate; potassium iodide; trichlorophosphate; In methanol; pentan-1-ol;
DOI:10.1016/j.bmc.2010.12.022