(1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate

Base Information

• Chemical Name: (1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate
• CAS No.: 1161147-26-7
• Molecular Formula: C₁₇H₂₂O₁₀
• Molecular Weight: 386.356

Synonyms:(1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate

Chemical Property of (1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate

Chemical Property:

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Technology Process of (1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate

There total 1 articles about (1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1R,4S,5S,6S)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)cyclohex-2-en-1-yl acetate (1161147-24-5) + acetic anhydride (108-24-7) → (1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate (1161147-26-7)

Guidance literature:

(1R,4S,5S,6S)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)cyclohex-2-en-1-yl acetate; With boron trichloride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

acetic anhydride; With pyridine; at 20 ℃; for 15h;

DOI:10.1021/ol9008987

Reference yield: 98.0%

(1R,2S,3S,4S)-5-(acetoxymethyl)cyclohex-5-ene-1,2,3,4-tetrayl tetraacetate (1161147-26-7) → (1R,2S,3S,4S)-5-(hydroxymethyl)cyclohex-5-ene-1,2,3,4-tetraol

Guidance literature:

With methanol; triethylamine; at 40 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ol9008987

upstream raw materials:

(1R,4S,5S,6S)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)cyclohex-2-en-1-yl acetate

acetic anhydride

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