Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI)
CAS No.:211996-00-8
Molecular Formula:C10H16 O
Molecular Weight:152.23344
Hs Code.:
Mol file:211996-00-8.mol

Synonyms:Cyclohexanecarboxaldehyde,4-(1Z)-1-propenyl-, trans- (9CI)

Suppliers and Price of Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI)

Chemical Property:

Boiling Point:212.5±29.0 °C(Predicted)
PSA：17.07000
Density:1.022±0.06 g/cm3(Predicted)
LogP:2.56780

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI)

There total 6 articles about Cyclohexanecarboxaldehyde, 4-(1Z)-1-propenyl-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 211995-98-1
trans-4-[(Z)-prop-1-en-1-yl]cyclohexanemethanol

: 211996-00-8,496949-27-0
trans-4-[(Z)-prop-1-en-1-yl]cyclohexanecarbaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -60 - 20 ℃;
DOI:10.1246/bcsj.71.1639

Reference yield:

: 3236-48-4
trans-1,4-Cyclohexanedimethanol

: 211996-00-8,496949-27-0
trans-4-[(Z)-prop-1-en-1-yl]cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 61 percent / pyridine / 2 h / 0 °C

2: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

3: 93 percent / tetrahydrofuran; hexane / 22 h / 0 - 20 °C

4: 99 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

5: 65 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

With pyridine; lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1: Esterification / 2: Swern oxidation / 3: Wittig reaction / 4: Reduction / 5: Swern oxidation;
DOI:10.1246/bcsj.71.1639

Reference yield:

: 211995-87-8
trans-4-(pivaloyloxymethyl)cyclohexanecarbaldehyde

: 211996-00-8,496949-27-0
trans-4-[(Z)-prop-1-en-1-yl]cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / tetrahydrofuran; hexane / 22 h / 0 - 20 °C

2: 99 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

3: 65 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1: Wittig reaction / 2: Reduction / 3: Swern oxidation;
DOI:10.1246/bcsj.71.1639