C₂₉H₄₄O₇

Base Information

Chemical Name:C₂₉H₄₄O₇
CAS No.:950598-39-7
Molecular Formula:C₂₉H₄₄O₇
Molecular Weight:504.664
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>7</sub>

Synonyms:C₂₉H₄₄O₇

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Chemical Property of C₂₉H₄₄O₇

Chemical Property:

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Technology Process of C₂₉H₄₄O₇

There total 19 articles about C₂₉H₄₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 950598-38-6
C₂₉H₄₄O₇

: 950598-39-7
C₂₉H₄₄O₇

Guidance literature:: With titanium(IV) isopropylate; In toluene; at 50 ℃; for 3h;
DOI:10.1021/ja073952e

Reference yield:

: 906624-11-1
(3S,6E)-8-(4-methoxybenzyloxy)-2,6-dimethylocta-1,6-dien-3-ol

: 950598-39-7
C₂₉H₄₄O₇

Guidance literature:: Multi-step reaction with 11 steps

1: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

2: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

3: DIBALH / CH₂Cl₂ / -78 °C

4: toluene / 80 °C

5: imidazole / CH₂Cl₂

6: DIBALH / CH₂Cl₂ / -78 °C

7: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

8: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

9: 63 percent / LDA / diethyl ether / -78 °C

10: 99 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

11: 40 percent / Ti(i-PrO)4 / toluene / 3 h / 50 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 4: Wittig reaction / 7: Sharpless asymmetric epoxidation;
DOI:10.1021/ja073952e

Reference yield:

: 906624-08-6
(2R,3S)-2-Iodomethyl-3-[(E)-5-(4-methoxy-benzyloxy)-3-methyl-pent-3-enyl]-2-methyl-oxirane

: 950598-39-7
C₂₉H₄₄O₇

Guidance literature:: Multi-step reaction with 12 steps

1: H₂O

2: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

3: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

4: DIBALH / CH₂Cl₂ / -78 °C

5: toluene / 80 °C

6: imidazole / CH₂Cl₂

7: DIBALH / CH₂Cl₂ / -78 °C

8: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

9: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

10: 63 percent / LDA / diethyl ether / -78 °C

11: 99 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

12: 40 percent / Ti(i-PrO)4 / toluene / 3 h / 50 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; tetrabutyl ammonium fluoride; water; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 5: Wittig reaction / 8: Sharpless asymmetric epoxidation;
DOI:10.1021/ja073952e