1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

Base Information

Chemical Name:1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol
CAS No.:88670-91-1
Molecular Formula:C₂₀H₃₀N₄O₃
Molecular Weight:374.483
Hs Code.:

Synonyms:1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

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Chemical Property of 1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

Chemical Property:

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Technology Process of 1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

There total 5 articles about 1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 88670-91-1
1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) DMF, 5 min, 2.) DMF, 60 deg C, 30 min

2: 69 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

3: 1.) sodium hydride / 1.) DMF, 5 min, 2.) DMF, 60 deg C, 30 min

4: ethanol / 18 h / Ambient temperature

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00370a012

Reference yield:

: 3351-59-5
2-(4-benzyloxyphenoxy)ethyl bromide

: 88670-91-1
1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) DMF, 5 min, 2.) DMF, 60 deg C, 30 min

2: 69 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

3: 1.) sodium hydride / 1.) DMF, 5 min, 2.) DMF, 60 deg C, 30 min

4: ethanol / 18 h / Ambient temperature

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00370a012

Reference yield:

: 80199-94-6
2-<2-<4-(benzyloxy)phenoxy>ethyl>-2H-benzotriazole

: 88670-91-1
1-Isopropylamino-3-{4-[2-(4,5,6,7-tetrahydro-benzotriazol-2-yl)-ethoxy]-phenoxy}-propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

2: 1.) sodium hydride / 1.) DMF, 5 min, 2.) DMF, 60 deg C, 30 min

3: ethanol / 18 h / Ambient temperature

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00370a012