5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

Base Information

Chemical Name:5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene
CAS No.:1242653-25-3
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:400.472
Hs Code.:

Synonyms:5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

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Chemical Property of 5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

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Technology Process of 5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

There total 2 articles about 5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 4-iodo-1-methoxy-2-(methoxymethoxy)benzene

: 1242653-07-1
(E)-N'-(cyclobutyl(3,4,5-trimethoxyphenyl)methylene)-4-methylbenzenesulfonohydrazide

: 1242653-25-3
5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); 1,3-bis-(diphenylphosphino)propane; caesium carbonate; In 1,4-dioxane; at 90 ℃; Inert atmosphere;
DOI:10.1021/ol101639g

Reference yield: 62.0%

: 1416990-98-1
C₂₁H₂₆N₂O₅S

: 1242653-25-3
5-(cyclobutylidene(4-methoxy-3-(methoxymethoxy)phenyl)methyl)-1,2,3-trimethoxybenzene

Guidance literature:: C₂₁H₂₆N₂O₅S; With dichloro bis(acetonitrile) palladium(II); 1,3-bis-(diphenylphosphino)propane; In 1,4-dioxane; at 20 ℃; for 0.0833333h; Inert atmosphere;

4-halo-1-methoxy-2-(methoxymethoxy)benzene; With caesium carbonate; In 1,4-dioxane; at 90 ℃; Inert atmosphere;
DOI:10.1039/c2ob26253c