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Technology Process of PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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  • Chemical Name:PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3
  • CAS No.:1337569-86-4
  • Molecular Formula:CF3O3S*C37H31Cl2N4P2Pd
  • Molecular Weight:920.024
  • Hs Code.:
PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>

Synonyms:PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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Chemical Property of PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3
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Technology Process of PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

There total 1 articles about PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

bis(benzonitrile)palladium(II) dichloride
15617-18-2,39958-10-6,14220-64-5

bis(benzonitrile)palladium(II) dichloride

(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-83-1

(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-86-4

PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

Guidance literature:
In tetrahydrofuran; (Ar, Schlenk) a mixt. of complex and diphosphine was dissolved in THF at-30°C, stirred at room temp. for 3 h; concd. under vac., the residue was washed with diethyl ether, recrystd. from CHCl3 at room temp.;
DOI:10.1021/ic201342z

Reference yield: 68.0%

dichloro bis(acetonitrile) palladium(II)
21264-30-2,90243-59-7,14592-56-4

dichloro bis(acetonitrile) palladium(II)

PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>NC<sub>3</sub>NH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=PdCl<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2N<sub>2</sub>C<sub>3</sub>H<sub>2</sub>CH<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)2)CF<sub>3</sub>SO<sub>3</sub>
1337569-86-4

PdCl2(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=PdCl2(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

C<sub>25</sub>H<sub>21</sub>Cl<sub>2</sub>N<sub>4</sub>PPd

C25H21Cl2N4PPd

Guidance literature:
With tetrabutyl-ammonium chloride; In acetonitrile; at 50 ℃; for 12h; Further stages; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejic.201500932
upstream raw materials:

bis(benzonitrile)palladium(II) dichloride

(C6H4NC3NH2P(C6H5)2N2C3H2CH3P(C6H5)2)(1+)*CF3SO3(1-)=(C6H4N2C3H2P(C6H5)2N2C3H2CH3P(C6H5)2)CF3SO3

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