2-[(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-N-ethylhydrazinecarbothioamide

Base Information

Chemical Name:2-[(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-N-ethylhydrazinecarbothioamide
CAS No.:512814-70-9
Molecular Formula:C₁₀H₁₇N₅OS
Molecular Weight:255.344
Hs Code.:
Mol file:512814-70-9.mol

Synonyms:1-[2-(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-4-ethylthiosemicarbazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-N-ethylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-[(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-N-ethylhydrazinecarbothioamide

There total 2 articles about 2-[(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-N-ethylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 542-85-8
Ethyl isothiocyanate

: 64019-58-5
α-(3,5-dimethyl-1-pyrazolyl)acetohydrazide

: 512814-70-9
1-[2-(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-4-ethylthiosemicarbazide

Guidance literature:: In ethanol; for 6h; Reflux;
DOI:10.1007/s00044-011-9691-4

Reference yield:

: 10199-60-7
ethyl 2-(3,5-dimethyl-1H-pyrazol-1-yl)acetate

: 512814-70-9
1-[2-(3,5-dimethyl-1H-pyrazol-1-yl)acetyl]-4-ethylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / Reflux

2: ethanol / 6 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1007/s00044-011-9691-4