Technology Process of 1,1'-[(1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diyl)diethoxy]-3,3',4,4'-tetraphenylferrocene
There total 1 articles about 1,1'-[(1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diyl)diethoxy]-3,3',4,4'-tetraphenylferrocene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Na2CO3 or K2CO3;
In
acetonitrile;
excess of Na2CO3, equimolar amts. of ferrocene-derivative and crown-ether, refluxing for 7 d; cooling, filtration, evapn., dissoln. (CH2Cl2), washing (H2O), sepn. org. layer, drying (MgSO4), filtration, evapn., chromy. (EtOAc:Et2NH 20:1);elem. anal.;
DOI:10.1021/om970681f