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C24H21Cl4N3O

Base Information
  • Chemical Name:C24H21Cl4N3O
  • CAS No.:1097079-02-1
  • Molecular Formula:C24H21Cl4N3O
  • Molecular Weight:509.262
  • Hs Code.:
C<sub>24</sub>H<sub>21</sub>Cl<sub>4</sub>N<sub>3</sub>O

Synonyms:C24H21Cl4N3O

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Chemical Property of C24H21Cl4N3O
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Technology Process of C24H21Cl4N3O

There total 4 articles about C24H21Cl4N3O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C29H29Cl4N3O3; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;
With sodium carbonate; In dichloromethane; water; Alkaline conditions;
With hydrogenchloride; borane-THF; sodium hydrogencarbonate; more than 3 stages;
Guidance literature:
Multi-step reaction with 3 steps
1.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 3 h / 20 °C / Reflux
1.2: 1.5 h / Reflux
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 48 h / 20 °C
3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
With carbonochloridic acid 1-chloro-ethyl ester; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;
Guidance literature:
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 48 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
upstream raw materials:

C29H29Cl4N3O3

C16H15Cl3N2

C17H18Cl4N2

Downstream raw materials:

C27H28Cl4N4O

C24H23Cl4N3

C25H25Cl4N3O2S

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