C₃₉H₅₆O₆Si

Base Information

Chemical Name:C₃₉H₅₆O₆Si
CAS No.:1320210-79-4
Molecular Formula:C₃₉H₅₆O₆Si
Molecular Weight:648.956
Hs Code.:

C<sub>39</sub>H<sub>56</sub>O<sub>6</sub>Si

Synonyms:C₃₉H₅₆O₆Si

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Chemical Property of C₃₉H₅₆O₆Si

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Technology Process of C₃₉H₅₆O₆Si

There total 12 articles about C₃₉H₅₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1320210-70-5
C₂₅H₂₈O₆

: 1320210-79-4
C₃₉H₅₆O₆Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

2.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

3.2: Saturated solution

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 60 °C / Inert atmosphere

5.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

7.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

8.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 1 h / 40 °C / Inert atmosphere

9.1: dimethyl sulfoxide / 3 h / 70 °C / Inert atmosphere

10.1: diisobutylaluminium hydride / hexane; dichloromethane / 2 h / -78 °C / Inert atmosphere

11.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

11.2: Saturated solution

With 1H-imidazole; titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; iodine; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: C₄₃H₆₆O₆Si₂

: 1320210-79-4
C₃₉H₅₆O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 1 h / 40 °C / Inert atmosphere

3.1: dimethyl sulfoxide / 3 h / 70 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 2 h / -78 °C / Inert atmosphere

5.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

5.2: Saturated solution

With 1H-imidazole; methanol; iodine; diisobutylaluminium hydride; triphenylphosphine; 10-camphorsulfonic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-75-0
C₃₁H₃₈O₆

: 1320210-79-4
C₃₉H₅₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

2.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 1 h / 40 °C / Inert atmosphere

4.1: dimethyl sulfoxide / 3 h / 70 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / hexane; dichloromethane / 2 h / -78 °C / Inert atmosphere

6.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

6.2: Saturated solution

With 1H-imidazole; methanol; iodine; diisobutylaluminium hydride; triphenylphosphine; 10-camphorsulfonic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2012.01.071