C₁₈H₂₂N₄O₄

Base Information

• Chemical Name: C₁₈H₂₂N₄O₄
• CAS No.: 1219733-88-6
• Molecular Formula: C₁₈H₂₂N₄O₄
• Molecular Weight: 358.397
• Mol file: 1219733-88-6.mol

Synonyms:C₁₈H₂₂N₄O₄

Chemical Property of C₁₈H₂₂N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₂N₄O₄

There total 1 articles about C₁₈H₂₂N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.1%

2-(3-nitro-6-aminophenoxy)ethanol (59820-41-6) + N,N-diethylaniline (91-66-7) → C18H22N4O4 (1219733-88-6)

Guidance literature:

2-(3-nitro-6-aminophenoxy)ethanol; With hydrogenchloride; In water; at 0 - 5 ℃;

N,N-diethylaniline; With sodium nitrite; In ethanol; water; at 5 ℃;

With sodium hydrogencarbonate; In ethanol; water; pH=7;

DOI:10.1016/j.dyepig.2009.09.008

Reference yield: 99.0%

C18H22N4O4 (1219733-88-6) + benzoic acid (65-85-0,8013-63-6) → C25H26N4O5 (1219733-89-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1016/j.dyepig.2009.09.008

Reference yield: 98.1%

1-naphthalenecarboxylic acid (86-55-5) + C18H22N4O4 (1219733-88-6) → C29H28N4O5 (1219733-90-0)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1016/j.dyepig.2009.09.008

upstream raw materials:

2-(3-nitro-6-aminophenoxy)ethanol

N,N-diethylaniline

Downstream raw materials:

C₃₂H₃₁N₅O₅

C₂₉H₂₈N₄O₅

C₂₅H₂₆N₄O₅

Refernces