C₃₁H₃₆BrNO₈

Base Information

Chemical Name:C₃₁H₃₆BrNO₈
CAS No.:1265221-64-4
Molecular Formula:C₃₁H₃₆BrNO₈
Molecular Weight:630.533
Hs Code.:

C<sub>31</sub>H<sub>36</sub>BrNO<sub>8</sub>

Synonyms:C₃₁H₃₆BrNO₈

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Chemical Property of C₃₁H₃₆BrNO₈

Chemical Property:

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Technology Process of C₃₁H₃₆BrNO₈

There total 14 articles about C₃₁H₃₆BrNO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1016650-10-4
2-(3-isopropoxy-4-methoxyphenyl)ethanol

: 1265221-63-3
C₁₉H₂₀BrNO₆

: 1265221-64-4
C₃₁H₃₆BrNO₈

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 18 ℃; for 1h;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1265221-55-3
C₈H₈INO₄

: 1265221-64-4
C₃₁H₃₆BrNO₈

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 14 h / 18 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide; 3: Mitsunobu reaction;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1265221-59-7
2-(3,4-diisopropoxyphenoxy)tetrahydro-2H-pyran

: 1265221-64-4
C₃₁H₃₆BrNO₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide; sodium carbonate / N,N-dimethyl-formamide / 3 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 12.66 h / -78 - 18 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran; hexane / 0.25 h

3.2: 24 h

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation

5.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 14 h / 18 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

With hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; water; sodium carbonate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide; 6.1: Mitsunobu reaction;
DOI:10.1002/ejoc.201001133