Technology Process of C24H17F3N4O6S2
There total 7 articles about C24H17F3N4O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
polyphosphoric acid trimethylsilyl ether;
at 160 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: caesium carbonate; copper(l) iodide; 2-Picolinic acid / 1,4-dioxane / 100 °C
2.1: sodium carbonate / N,N-dimethyl-formamide / 50 - 60 °C
3.1: sodium hydroxide; water / 1 h / 100 °C
3.2: pH ~ 1 / Cooling with ice
4.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 20 °C / Cooling with salt-ice; Cooling with ice
4.2: 20 °C / Cooling with ice; Cooling with salt-ice
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C
5.2: 2 h / 0 - 20 °C
6.1: Dowthern A / 0.17 h / 160 °C
7.1: polyphosphoric acid trimethylsilyl ether / 160 °C
With
2-Picolinic acid; copper(l) iodide; water; sodium hydride; sodium carbonate; caesium carbonate; 1,1'-carbonyldiimidazole; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C
1.2: 2 h / 0 - 20 °C
2.1: Dowthern A / 0.17 h / 160 °C
3.1: polyphosphoric acid trimethylsilyl ether / 160 °C
With
sodium hydride;
In
tetrahydrofuran; mineral oil;