4-Morpholino-2,3,5,6-tetrachloropyridine

Base Information

Chemical Name:4-Morpholino-2,3,5,6-tetrachloropyridine
CAS No.:2176-66-1
Molecular Formula:C₉H₈Cl₄N₂O
Molecular Weight:301.987
Hs Code.:
European Community (EC) Number:663-218-0

Synonyms:4-MORPHOLINO-2,3,5,6-TETRACHLOROPYRIDINE;4-(Perchloropyridin-4-yl)morpholine;AKOS024340139

Suppliers and Price of 4-Morpholino-2,3,5,6-tetrachloropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Morpholino-2,3,5,6-tetrachloropyridine

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:301.936124
Heavy Atom Count:16
Complexity:226

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1COCCN1C2=C(C(=NC(=C2Cl)Cl)Cl)Cl

Technology Process of 4-Morpholino-2,3,5,6-tetrachloropyridine

There total 2 articles about 4-Morpholino-2,3,5,6-tetrachloropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 110-91-8,99108-56-2
morpholine

: 13239-90-2
2,3,5,6-tetrachloro-4-(phenylsulfonyl)pyridine

: 4-(3,5,6-trichloro-4-(phenylsulfonyl)pyridin-2-yl)morpholine

: 2176-66-1
4-(perchloropyridin-4-yl)morpholine

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1007/s13738-016-1043-3

Reference yield:

: 2176-62-7
2,3,4,5,6-pentachloropyridine

: 4-(3,5,6-trichloro-4-(phenylsulfonyl)pyridin-2-yl)morpholine

: 2176-66-1
4-(perchloropyridin-4-yl)morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 10 h / 20 °C

2: potassium carbonate / acetonitrile / 4 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s13738-016-1043-3