C₄₀H₅₄O₅Si

Base Information

Chemical Name:C₄₀H₅₄O₅Si
CAS No.:1365268-46-7
Molecular Formula:C₄₀H₅₄O₅Si
Molecular Weight:642.951
Hs Code.:

C<sub>40</sub>H<sub>54</sub>O<sub>5</sub>Si

Synonyms:C₄₀H₅₄O₅Si

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Chemical Property of C₄₀H₅₄O₅Si

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Technology Process of C₄₀H₅₄O₅Si

There total 7 articles about C₄₀H₅₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1365268-32-1
C₄₁H₅₄O₆Si

: 1365268-46-7
C₄₀H₅₄O₅Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₁₉H₂₄O₂

: 1365268-46-7
C₄₀H₅₄O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

3.2: 0 °C

3.3: -78 °C

4.1: 1H-imidazole / dichloromethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

6.1: diisobutylaluminium hydride / dichloromethane / -78 °C

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₂₅H₃₅NO

: 1365268-46-7
C₄₀H₅₄O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid; orthoformic acid triethyl ester / benzene / 20 °C

2.1: toluene-4-sulfonic acid / benzene / Reflux

3.1: n-butyllithium / tetrahydrofuran / -78 °C

3.2: -78 - 20 °C

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

4.2: 0 °C

4.3: -78 °C

5.1: 1H-imidazole / dichloromethane / 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

7.1: diisobutylaluminium hydride / dichloromethane / -78 °C

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; orthoformic acid triethyl ester; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2012.01.058