2-benzyl-5-methylisoindoline

Base Information

Chemical Name:2-benzyl-5-methylisoindoline
CAS No.:97754-25-1
Molecular Formula:C₁₆H₁₇N
Molecular Weight:223.318
Hs Code.:

Synonyms:2-benzyl-5-methylisoindoline

Suppliers and Price of 2-benzyl-5-methylisoindoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-5-methylisoindoline

Chemical Property:

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Technology Process of 2-benzyl-5-methylisoindoline

There total 3 articles about 2-benzyl-5-methylisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 92855-70-4
2-benzyl-5-methylisoindoline-1,3-dione

: 97754-25-1
2-benzyl-5-methylisoindoline

Guidance literature:: With 1,1,3,3-Tetramethyldisiloxane; tris(pentafluorophenyl)borate; In 1,4-dioxane; at 110 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2018.01.051

Reference yield:

: 19438-61-0
4-methylphthalic anhydride

: 100-46-9
benzylamine

: 97754-25-1
2-benzyl-5-methylisoindoline

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 3 h / Reflux; Inert atmosphere; Schlenk technique

2: tris(pentafluorophenyl)borate; 1,1,3,3-Tetramethyldisiloxane / 1,4-dioxane / 16 h / 110 °C / Inert atmosphere; Schlenk technique

With 1,1,3,3-Tetramethyldisiloxane; tris(pentafluorophenyl)borate; acetic acid; In 1,4-dioxane;
DOI:10.1016/j.tet.2018.01.051