9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

Base Information

Chemical Name:9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one
CAS No.:1313021-95-2
Molecular Formula:C₁₇H₂₁NO
Molecular Weight:255.36
Hs Code.:

Synonyms:9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

Suppliers and Price of 9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

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Technology Process of 9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

There total 4 articles about 9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 933727-25-4
9-amino-6,7,8,9-tetrahydro-benzocyclohepten-5-one

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 1313021-95-2
9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

Guidance literature:: With triethylamine; In dichloromethane; for 12h; Reflux;
DOI:10.2174/157340611795564222

Reference yield:

: C₁₆H₂₁NO₃

: 1313021-95-2
9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

2: triethylamine / dichloromethane / 12 h / Reflux

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.2174/157340611795564222

Reference yield:

: 1351997-24-4
C₁₁H₁₁N₃O

: 1313021-95-2
9-(cyclohex-2-en-1-ylamino)-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

3: triethylamine / dichloromethane / 12 h / Reflux

With palladium 10% on activated carbon; hydrogen; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane; ethyl acetate;
DOI:10.2174/157340611795564222