octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

Base Information

Chemical Name:octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside
CAS No.:900523-87-7
Molecular Formula:C₆₈H₈₄O₁₉
Molecular Weight:1205.4
Hs Code.:

Synonyms:octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

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Chemical Property of octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

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Technology Process of octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

There total 6 articles about octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 900523-86-6
octyl 2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,5-di-O-benzyl-α-D-arabinofuranoside

: 32934-24-0,41670-79-5,52645-73-5,55722-49-1,79389-52-9,99031-86-4,125354-48-5,126187-25-5
S-ethyl 2,3,4,6-tetra-O-acetyl-1-deoxy-1-thio-α-D-mannopyranoside

: 900523-87-7
octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1139/V06-049

Reference yield:

: 900523-84-4
octyl 2,3-anhydro-5-O-benzyl-α-D-lyxofuranoside

: 900523-87-7
octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / phenylmethanol / 100 °C

2: 84 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 3.5 h / -40 - 20 °C

3: 97 percent / K₂CO₃ / methanol / 20 °C

4: 61 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 4 h / 0 - 20 °C

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; potassium carbonate; In methanol; dichloromethane; benzyl alcohol;
DOI:10.1139/V06-049

Reference yield:

: 900523-83-3
octyl 3,5-di-O-benzyl-α-D-arabinofuranoside

: 900523-87-7
octyl 2-O-[2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-3,5-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 3.5 h / -40 - 20 °C

2: 97 percent / K₂CO₃ / methanol / 20 °C

3: 61 percent / molecular sieves 4 Angstroem; N-iodosuccinimide; silver triflate / CH₂Cl₂ / 4 h / 0 - 20 °C

With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; potassium carbonate; In methanol; dichloromethane;
DOI:10.1139/V06-049