N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide
• CAS No.: 1146970-53-7
• Molecular Formula: C₂₀H₂₅NO₃S
• Molecular Weight: 359.489
• Mol file: 1146970-53-7.mol

Synonyms:N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide

Chemical Property of N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H19NO (1146970-66-2) + p-toluenesulfonyl chloride (98-59-9) → N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide (1146970-53-7)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ol9003492

Reference yield:

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) + N-(3-(2-methoxybenzyl)pent-4-enyl)-4-methylbenzenesulfonamide (1146970-53-7) → cis-1-((3-(2-methoxybenzyl)-1-tosylpyrrolidin-2-yl)methoxy)-2,2,6,6-tetramethylpiperidine + trans-1-((3-(2-methoxybenzyl)-1-tosylpyrrolidin-2-yl)methoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:

With copper(II) 2-ethylhexanoate; caesium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 24h; optical yield given as %de; diastereoselective reaction;

DOI:10.1021/ol9003492

upstream raw materials:

C₁₃H₁₉NO

p-toluenesulfonyl chloride