methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

Base Information

Chemical Name:methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate
CAS No.:934762-85-3
Molecular Formula:C₂₂H₂₁NO₇
Molecular Weight:411.411
Hs Code.:

Synonyms:methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

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Technology Process of methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

There total 1 articles about methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 553-90-2
Dimethyl oxalate

: 934762-83-1
3-(3,4-dimethoxycinnamoylamino)acetophenone

: 934762-85-3
methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

Guidance literature:: Dimethyl oxalate; 3-(3,4-dimethoxycinnamoylamino)acetophenone; With sodium methylate; In tetrahydrofuran; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1021/jm1010594

Reference yield: 62.0%

: 934762-85-3
methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate

: 934762-93-3
4-(3-caffeoylaminophenyl)-2-hydroxy-4-oxo-2-butenoic acid

Guidance literature:: methyl 4-(3-(3,4-dimethoxycinnamoylamino)phenyl)-2-hydroxy-4-oxo-2-butenoate; With boron tribromide; In dichloromethane; at 20 ℃; Reflux;

With water; In dichloromethane; at -78 ℃;
DOI:10.1021/jm1010594