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5-bromo-4-methoxy-3-phenylfuran-2(5H)-one

Base Information Edit
  • Chemical Name:5-bromo-4-methoxy-3-phenylfuran-2(5H)-one
  • CAS No.:100074-67-7
  • Molecular Formula:C11H9BrO3
  • Molecular Weight:269.095
  • Hs Code.:
  • Mol file:100074-67-7.mol
5-bromo-4-methoxy-3-phenylfuran-2(5H)-one

Synonyms:5-bromo-4-methoxy-3-phenylfuran-2(5H)-one

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Chemical Property of 5-bromo-4-methoxy-3-phenylfuran-2(5H)-one Edit
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Technology Process of 5-bromo-4-methoxy-3-phenylfuran-2(5H)-one

There total 6 articles about 5-bromo-4-methoxy-3-phenylfuran-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In 1,2-dichloro-ethane; for 2h; Heating;
DOI:10.1039/P19850001567
Guidance literature:
Multi-step reaction with 3 steps
1: sodium ethoxide / ethanol / 1.5 h / Ambient temperature
2: 424 g / potassium carbonate / acetone / 1 h / Heating
3: 86 percent / azoisobutyronitrile, N-bromosuccinimide / 1,2-dichloro-ethane / 2 h / Heating
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; sodium ethanolate; In ethanol; 1,2-dichloro-ethane; acetone;
DOI:10.1039/P19850001567
Guidance literature:
Multi-step reaction with 4 steps
1: 774 g / sodium ethoxide / ethanol / 4 h / Heating
2: 446 g / potassium t-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
3: 424 g / potassium carbonate / acetone / 1 h / Heating
4: 86 percent / azoisobutyronitrile, N-bromosuccinimide / 1,2-dichloro-ethane / 2 h / Heating
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium tert-butylate; sodium ethanolate; potassium carbonate; In ethanol; 1,2-dichloro-ethane; acetone; tert-butyl alcohol;
DOI:10.1039/P19850001567
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