(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

Base Information

Chemical Name:(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole
CAS No.:1186031-22-0
Molecular Formula:C₂₁H₂₇NO₂S
Molecular Weight:357.517
Hs Code.:

Synonyms:(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

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Technology Process of (3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

There total 3 articles about (3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1186031-01-5
(E)-N-(3-cyclohexylideneallyl)-4-methyl-N-(penta-2,4-dien-1-yl)benzenesulfonamide

: 1186031-22-0
(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

Guidance literature:: With silver hexafluoroantimonate; C₆₄H₄₆AuClNO₂P; In dichloromethane; at -15 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja905415r

Reference yield: 88.0%

: C₁₈H₂₃NO₂S

: 1186031-22-0
(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

Guidance literature:: With silver tetrafluoroborate; C₅₀H₅₄AuClNO₄P; In dichloromethane; at 0 - 20 ℃; for 1.91667h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja303641p

Reference yield:

: 1186031-01-5
(E)-N-(3-cyclohexylideneallyl)-4-methyl-N-(penta-2,4-dien-1-yl)benzenesulfonamide

: 1186031-22-0
(3aS,7aR)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

: 1186031-26-4
(3aR,7aS)-4-cyclohexylidene-2-(p-tosyl)-2,3,3a,4,5,7a-hexahydro-1H-isoindole

Guidance literature:: With silver hexafluoroantimonate; C₄₈H₃₈AuClNO₂P; In dichloromethane; at -15 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja905415r