2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid

Base Information

• Chemical Name: 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid
• CAS No.: 142270-32-4
• Molecular Formula: C₁₀₂H₉₅ClF₃NO₃₀
• Molecular Weight: 1907.31
• Mol file: 142270-32-4.mol

Synonyms:2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid

Chemical Property of 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid

There total 1 articles about 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl bromide (142270-36-8) + 2-(4-trifluoroacetamidophenyl)ethyl O-<6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl>-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-manno-heptopyranoside (142270-31-3) → 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid (142270-32-4)

Guidance literature:

With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; toluene; for 5h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90553-6

Reference yield: 64.0%

2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-mannoheptopyranosyl>-(1-7)-O-(6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-mannoheptopyranosid (142270-32-4) → 2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl>-(1-7)-O-(6-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-manno-heptopyranoside (142270-33-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h; under 3000.2 Torr;

DOI:10.1016/S0008-6215(00)90553-6

upstream raw materials:

2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl bromide

2-(4-trifluoroacetamidophenyl)ethyl O-<6-O-benzoyl-2,3,4-tri-O-benzyl-L-glycero-α-D-manno-heptopyranosyl>-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-manno-heptopyranoside

Downstream raw materials:

2-(4-trifluoroacetamidophenyl)ethyl O-<2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl>-(1-7)-O-(6-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl)-(1-3)-2,6,7-tri-O-acetyl-4-O-chloroacetyl-L-glycero-α-D-manno-heptopyranoside