C₃₈H₅₂O₂Si₃

Base Information

• Chemical Name: C₃₈H₅₂O₂Si₃
• CAS No.: 410531-52-1
• Molecular Formula: C₃₈H₅₂O₂Si₃
• Molecular Weight: 625.086
• Mol file: 410531-52-1.mol

Synonyms:C₃₈H₅₂O₂Si₃

Chemical Property of C₃₈H₅₂O₂Si₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₅₂O₂Si₃

There total 1 articles about C₃₈H₅₂O₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

diphenylsilyl dichloride (80-10-4) + [(3-bromobenzyl)oxy](tert-butyl)dimethylsilane (103978-12-7) → C38H52O2Si3 (410531-52-1)

Guidance literature:

[(3-bromobenzyl)oxy](tert-butyl)dimethylsilane; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 0.5h;

diphenylsilyl dichloride; In diethyl ether; pentane; at -78 - 20 ℃; Further stages.;

DOI:10.1002/1521-3765(20020104)8:1<45::AID-CHEM45>3.0.CO;2-P

Reference yield: 89.0%

C38H52O2Si3 (410531-52-1) → {3-[(3-hydroxymethyl-phenyl)-diphenyl-silanyl]-phenyl}-methanol (410531-53-2)

Guidance literature:

With acetic acid; In tetrahydrofuran; at 50 ℃; for 3h;

DOI:10.1002/1521-3765(20020104)8:1<45::AID-CHEM45>3.0.CO;2-P

Reference yield:

C38H52O2Si3 (410531-52-1) → bis-(3-bromomethyl-phenyl)-diphenyl-silane (410531-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / aq. AcOH / tetrahydrofuran / 3 h / 50 °C

2: 91 percent / PBr₃ / benzene / 3 h / 20 °C

With phosphorus tribromide; acetic acid; In tetrahydrofuran; benzene;

DOI:10.1002/1521-3765(20020104)8:1<45::AID-CHEM45>3.0.CO;2-P

upstream raw materials:

diphenylsilyl dichloride

[(3-bromobenzyl)oxy](tert-butyl)dimethylsilane

Downstream raw materials:

{3-[(3-hydroxymethyl-phenyl)-diphenyl-silanyl]-phenyl}-methanol

bis-(3-bromomethyl-phenyl)-diphenyl-silane

C₃₆H₃₅BrN₂OSi

C₄₂H₄₉BrN₂OSi₂

Refernces