Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-

Base Information

Chemical Name:Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-
CAS No.:142439-16-5
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:204.273
Hs Code.:
DSSTox Substance ID:DTXSID301260686

Synonyms:Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-;DTXSID301260686;142439-16-5

Suppliers and Price of Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:204.134369001
Heavy Atom Count:15
Complexity:203

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(CC1)CC(=O)C2=CC=CC=C2
Isomeric SMILES:C1CCN(CC1)C[13C](=O)C2=CC=CC=C2

Technology Process of Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)-

There total 2 articles about Ethanone-1-13C, 1-phenyl-2-(1-piperidinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10383-88-7
acetophenone-13C=O

: 142439-16-5
2-(1-piperidinyl)acetophenone-13C

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / (C₄H₉)4NBr₃ / CH₂Cl₂; methanol / Ambient temperature

2: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h, 2.) ether, hexane, RT, overnight

With n-butyllithium; tetra-N-butylammonium tribromide; In methanol; dichloromethane;
DOI:10.1021/ja00044a010

Reference yield:

: 110-89-4
piperidine

: 622787-74-0
2-bromo-1-¹³C-phenylethanone

: 142439-16-5
2-(1-piperidinyl)acetophenone-13C

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, RT, 1 h, 2.) ether, hexane, RT, overnight;
DOI:10.1021/ja00044a010

Reference yield: 90.0%

: 142439-16-5
2-(1-piperidinyl)acetophenone-13C

: 142439-17-6
C₁₂⁽¹³⁾CH₁₇NO

Guidance literature:: With dicobalt octacarbonyl; dodecacarbonyl-triangulo-triruthenium; carbon monoxide; In benzene; at 200 - 220 ℃; for 72h; under 41040 Torr;
DOI:10.1021/ja00044a010