allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside
CAS No.:1117751-18-4
Molecular Formula:C₅₁H₆₀O₂₆
Molecular Weight:1089.02
Hs Code.:

Synonyms:allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

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Chemical Property of allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

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Technology Process of allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

There total 1 articles about allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 121238-27-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate

: 314038-22-7
allyl 2,4-di-O-benzoyl-α-D-mannopyranoside

: 1117751-18-4
allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2008.11.004

Reference yield: 74.0%

: 1117751-18-4
allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

: 904690-07-9
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranose

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; at 80 ℃; for 1h;
DOI:10.1016/j.bmc.2008.11.004

Reference yield:

: 1117751-18-4
allyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl]-(1->6)-2,4-di-O-benzoyl-α-D-mannopyranoside

: 904690-08-0
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->3)-[2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl-(1->6)-]-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid / 1 h / 80 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/j.bmc.2008.11.004