C₂₁H₃₁NO₆

Base Information

Chemical Name:C₂₁H₃₁NO₆
CAS No.:1393106-02-9
Molecular Formula:C₂₁H₃₁NO₆
Molecular Weight:393.48
Hs Code.:

C<sub>21</sub>H<sub>31</sub>NO<sub>6</sub>

Synonyms:C₂₁H₃₁NO₆

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Chemical Property of C₂₁H₃₁NO₆

Chemical Property:

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Technology Process of C₂₁H₃₁NO₆

There total 10 articles about C₂₁H₃₁NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1393106-19-8
tert-butyl 2-(benzyloxymethyl)-3,4-O-isopropylidene-5-(tert-butyldiphenylsilyloxy)piperidine-1-carboxylate

: 1393106-02-9
C₂₁H₃₁NO₆

Guidance literature:: tert-butyl 2-(benzyloxymethyl)-3,4-O-isopropylidene-5-(tert-butyldiphenylsilyloxy)piperidine-1-carboxylate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h; Inert atmosphere;

With water;
DOI:10.1002/ejoc.201200377

Reference yield:

: 1241959-31-8
tert-butyl (R)-1-(benzyloxy)but-3-en-2-yl((R,E)-2-(tert-butyldiphenylsilyloxy)pent-3-enyl)carbamate

: 1393106-02-9
C₂₁H₃₁NO₆

Guidance literature:: Multi-step reaction with 8 steps

1: Grubbs catalyst first generation / dichloromethane / 48 h / Reflux; Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Cooling with ice

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / -75 °C / Inert atmosphere

4: water; sodium hydroxide / methanol / 3 h / 0 - 20 °C / Inert atmosphere

5: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

6: potassium osmate(VI) dihydrate; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 48 h / -10 °C / Inert atmosphere

7: boron trifluoride diethyl etherate / tetrahydrofuran; acetone / 1 h / 5 - 20 °C / Cooling with ice

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / Inert atmosphere

With 1H-imidazole; Grubbs catalyst first generation; potassium osmate(VI) dihydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; 3: Mitsunobu reaction;
DOI:10.1002/ejoc.201200377

Reference yield:

: 1241959-30-7
(R,E)-N-((R)-1-(benzyloxy)but-3-en-2-yl)-2-(tert-butyldiphenylsilyloxy)pent-3-en-1-amine

: 1393106-02-9
C₂₁H₃₁NO₆

Guidance literature:: Multi-step reaction with 9 steps

1: triethylamine / tetrahydrofuran / 20 h / 50 °C / Inert atmosphere

2: Grubbs catalyst first generation / dichloromethane / 48 h / Reflux; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Cooling with ice

4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / -75 °C / Inert atmosphere

5: water; sodium hydroxide / methanol / 3 h / 0 - 20 °C / Inert atmosphere

6: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

7: potassium osmate(VI) dihydrate; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 48 h / -10 °C / Inert atmosphere

8: boron trifluoride diethyl etherate / tetrahydrofuran; acetone / 1 h / 5 - 20 °C / Cooling with ice

9: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / Inert atmosphere

With 1H-imidazole; Grubbs catalyst first generation; potassium osmate(VI) dihydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; 4: Mitsunobu reaction;
DOI:10.1002/ejoc.201200377