(3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane

Base Information

• Chemical Name: (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane
• CAS No.: 1384525-54-5
• Molecular Formula: C₃₆H₃₉NO₆
• Molecular Weight: 581.709

Synonyms:(3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane

Chemical Property of (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane

Chemical Property:

Purity/Quality:

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Technology Process of (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane

There total 3 articles about (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C43H45NO9S → (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane (1384525-54-5)

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.carres.2011.10.039

Reference yield:

(4R,5S,6S)-N-benzyloxycarbonyl-3-methylene-4,5,6-tribenzyloxyazepane → (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane (1384525-54-5)

Guidance literature:

Multi-step reaction with 3 steps

1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

2: pyridine / 24 h / 0 - 20 °C / Inert atmosphere

3: lithium triethylborohydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With pyridine; osmium(VIII) oxide; lithium triethylborohydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; acetone; tert-butyl alcohol;

DOI:10.1016/j.carres.2011.10.039

Reference yield:

C36H39NO7 (1384525-50-1) → (3R,4S,5R,6S)-N-benzyloxycarbonyl-3-hydroxy-3-methyl-4,5,6-tribenzyloxyazepane (1384525-54-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 24 h / 0 - 20 °C / Inert atmosphere

2: lithium triethylborohydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With pyridine; lithium triethylborohydride; In tetrahydrofuran;

DOI:10.1016/j.carres.2011.10.039

upstream raw materials:

C₃₆H₃₉NO₇

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