phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Base Information

Chemical Name:phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside
CAS No.:744193-99-5
Molecular Formula:C₃₂H₄₅Cl₃N₂O₁₉S
Molecular Weight:900.136
Hs Code.:

phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Synonyms:phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

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Chemical Property of phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

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Technology Process of phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

There total 5 articles about phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 55569-66-9
cytidine 5'-monophosphate-N-acetylneuraminic acid

: 512174-10-6
phenyl O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

: 744193-99-5
phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: With sialyltransferase FUS-01/2; magnesium chloride; In various solvent(s); at 37 ℃; for 2h; pH=6.0; Enzymatic reaction;
DOI:10.1021/jo026569v

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 744193-99-5
phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / H₂O

1.2: pyridine

1.3: BF₃*Et₂O

2.1: 1M HCl / ethanol

3.1: 89 percent / UDP-galactose 4-epimerase/β(1-4)galactosyltransferase; MnCl2 / various solvent(s) / 20 h / 37 °C / pH 7.4 / Enzymatic reaction

4.1: 94 percent / MgCl₂; sialyltransferase FUS-01/2 / various solvent(s) / 2 h / 37 °C / pH 6.0 / Enzymatic reaction

With hydrogenchloride; UDP-galactose 4-epimerase; β(1-4)galactosyltransferase; sialyltransferase FUS-01/2; potassium carbonate; magnesium chloride; manganese(ll) chloride; In ethanol; water;
DOI:10.1021/jo026569v

Reference yield:

: 108-98-5
thiophenol

: 744193-99-5
phenyl O-(5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2-3)-O-(β-D-galactopyranosyl)-(1-4)-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / H₂O

1.2: pyridine

1.3: BF₃*Et₂O

2.1: 1M HCl / ethanol

3.1: 89 percent / UDP-galactose 4-epimerase/β(1-4)galactosyltransferase; MnCl2 / various solvent(s) / 20 h / 37 °C / pH 7.4 / Enzymatic reaction

4.1: 94 percent / MgCl₂; sialyltransferase FUS-01/2 / various solvent(s) / 2 h / 37 °C / pH 6.0 / Enzymatic reaction

With hydrogenchloride; UDP-galactose 4-epimerase; β(1-4)galactosyltransferase; sialyltransferase FUS-01/2; potassium carbonate; magnesium chloride; manganese(ll) chloride; In ethanol; water;
DOI:10.1021/jo026569v