4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

Base Information

Chemical Name:4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid
CAS No.:103751-39-9
Molecular Formula:C₃₅H₃₉BrN₆O₈
Molecular Weight:751.634
Hs Code.:

Synonyms:4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

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Chemical Property of 4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

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Technology Process of 4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

There total 1 articles about 4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1,4-Di-O-acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α,β-L-galactopyranose

: 103751-39-9
4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

Guidance literature:: With titanium(IV) bromide; In dichloromethane; ethyl acetate; for 1h; Ambient temperature;

Reference yield:

: 108-24-7
acetic anhydride

: 103751-39-9
4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

: 103833-25-6
Benzyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

: 103751-41-3
Benzyl-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(4-O-acetyl-2-azido-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

: 103833-26-7
Benzyl-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(4-O-acetyl-2-azido-2,6-didesoxy-β-L-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

: 103751-39-9
4-O-Acetyl-2-azido-3-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-2,6-didesoxy-α-L-galactopyranosylbromid

: 103751-42-4
Benzyl-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-mannopyranosyl)-(1->3)-O-(2-acetamido-4-O-acetyl-2,6-didesoxy-α-L-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

Guidance literature:: Multi-step reaction with 2 steps

2: 1) H₂S-gas / 1.) pyridine, H₂O, 18h, r.t. 2.) pyridine, 0 deg C, 6h

With hydrogen sulfide;