Technology Process of C46H70O16
There total 52 articles about C46H70O16 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: 96 percent / DMAP; pyridine / tetrahydrofuran
2: 100 percent / 1-methyl-1,4-cyclohexadiene; CaCO3 / Pd(OH)2/C / ethanol
3: 87 percent / iPr2NEt / CH2Cl2
4: 88 percent / Dess-Martin periodinane; pyridine / CH2Cl2
5: HF / acetonitrile / 0 °C
With
pyridine; dmap; 2,5-dihydrotoluene; hydrogen fluoride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; calcium carbonate;
palladium dihydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/1521-3773(20010105)40:1<191::AID-ANIE191>3.0.CO;2-C
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 91 percent / imidazole / dimethylformamide
2: 82 percent / aq. HClO4 / CH2Cl2
3: 95 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinine / CH2Cl2; H2O / 0 °C
4: 96 percent / DMAP; pyridine / tetrahydrofuran
5: 100 percent / 1-methyl-1,4-cyclohexadiene; CaCO3 / Pd(OH)2/C / ethanol
6: 87 percent / iPr2NEt / CH2Cl2
7: 88 percent / Dess-Martin periodinane; pyridine / CH2Cl2
8: HF / acetonitrile / 0 °C
With
pyridine; 1H-imidazole; dmap; perchloric acid; 2,5-dihydrotoluene; hydrogen fluoride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate;
palladium dihydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/1521-3773(20010105)40:1<191::AID-ANIE191>3.0.CO;2-C