C₁₃H₁₃NO₃Si

Base Information

• Chemical Name: C₁₃H₁₃NO₃Si
• CAS No.: 1232394-75-0
• Molecular Formula: C₁₃H₁₃NO₃Si
• Molecular Weight: 259.337
• Mol file: 1232394-75-0.mol

Synonyms:C₁₃H₁₃NO₃Si

Chemical Property of C₁₃H₁₃NO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₃NO₃Si

There total 1 articles about C₁₃H₁₃NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylsilane (694-53-1) + 4-nitrobenzaldehdye (555-16-8) → C13H13NO3Si (1232394-75-0)

Guidance literature:

With (CH₃NC₃H₂NCH(C₆H₅)CH₂C₅(CH₃)4)FeCl; In acetonitrile; at 80 ℃; for 2h; Inert atmosphere;

DOI:10.1021/om100246j

Reference yield: 92.0%

C13H13NO3Si (1232394-75-0) → 4-nitrobenzyl chloride (619-73-8)

Guidance literature:

With sodium hydroxide; In water; Schlenk technique; Inert atmosphere;

DOI:10.1007/s10562-021-03578-9

upstream raw materials:

phenylsilane

4-nitrobenzaldehdye

Downstream raw materials:

4-nitrobenzyl chloride

Refernces

• 1、 Chang, Jiarui,Fang, Fei,Zhang, Jie,Chen, Xuenian. "Hydrosilylation of Aldehydes and Ketones Catalysed by Bis(phosphinite) Pincer Platinum Hydride Complexes". . p. 2709 - 2715. Retrieved 2020/06/02.
• 2、 Kandepi, V. V. Krishna Mohan,Cardoso, Joao M. S.,Peris, Eduardo,Royo, Beatriz. "Iron(II) complexes bearing chelating cyclopentadienyl-N-heterocyclic carbene ligands as catalysts for hydrosilylation and hydrogen transfer reactions". experimental part. p. 2777 - 2782. Retrieved 2010/08/06.