1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

Base Information

Chemical Name:1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone
CAS No.:1401430-12-3
Molecular Formula:C₁₇H₁₇BrI₂N₂Se
Molecular Weight:662.008
Hs Code.:

Synonyms:1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

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Chemical Property of 1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

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Technology Process of 1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

There total 4 articles about 1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1401430-03-2
C₁₇H₁₇BrN₂Se

: 1401430-12-3
1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

Guidance literature:: With iodine; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.07.025

Reference yield:

: 1401429-98-8
3-(2-bromobenzyl)-1-isopropyl-1H-benzo[d]imidazol-3-ium bromide

: 1401430-12-3
1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium diselenide / tetrahydrofuran / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: iodine / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With sodium diselenide; iodine; In tetrahydrofuran;
DOI:10.1016/j.jorganchem.2012.07.025

Reference yield:

: 17583-50-5
N-isopropylbenzimidazole

: 1401430-12-3
1-(2-bromobenzyl)-3-isopropyl-1H-benzo[d]imidazole-2(3H)-diiodoselone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 16 h / Inert atmosphere; Reflux

2.1: sodium diselenide / tetrahydrofuran / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: iodine / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With sodium diselenide; iodine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/j.jorganchem.2012.07.025