(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

Base Information

Chemical Name:(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid
CAS No.:958489-40-2
Molecular Formula:C₁₅H₁₈ClF₃N₂O₄S
Molecular Weight:414.833
Hs Code.:

Synonyms:(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

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Chemical Property of (2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

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Technology Process of (2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

There total 3 articles about (2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 958489-39-9
(2R)-2-tert-butoxycarbonylamino-3-(2-chloro-6-nitro-4-trifluoromethylphenylsulfanyl)propionic acid

: 958489-40-2
(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 5.5h; under 3800.26 Torr;

Reference yield:

: 101646-02-0
5-Chloro-4-fluoro-3-nitro-trifluoromethylbenzene

: 958489-40-2
(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / ethanol; water / 2 h / Heating / reflux

1.2: pH 2 - 3

2.1: hydrogen / palladium 10% on activated carbon / methanol / 5.5 h / 20 °C / 3800.26 Torr

With hydrogen; sodium hydrogencarbonate; palladium 10% on activated carbon; In methanol; ethanol; water;

Reference yield:

: 20887-95-0
N-(tert-Butyloxycarbonyl)-L-cysteine

: 958489-40-2
(2R)-3-(2-amino-6-chloro-4-trifluoromethylphenylsulfanyl)-2-tert-butoxycarbonylaminopropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / ethanol; water / 2 h / Heating / reflux

1.2: pH 2 - 3

2.1: hydrogen / palladium 10% on activated carbon / methanol / 5.5 h / 20 °C / 3800.26 Torr

With hydrogen; sodium hydrogencarbonate; palladium 10% on activated carbon; In methanol; ethanol; water;