5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

Base Information

Chemical Name:5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile
CAS No.:329326-24-1
Molecular Formula:C₂₀H₁₁N₅O₃
Molecular Weight:369.339
Hs Code.:

Synonyms:5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

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Chemical Property of 5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

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Technology Process of 5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

There total 1 articles about 5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 206268-72-6
4-bromo-5-nitrophthalonitrile

: 1689-82-3
4-hydroxyazobenzene

: 329326-24-1
5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

Guidance literature:: With lithium hydroxide; In dimethyl sulfoxide; at 20 - 25 ℃; for 168h;

Reference yield: 18.0%

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 329326-24-1
5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

: 329246-19-7
cobalt tetra-5-nitrotetra-4-((4-phenylazo)phenoxy)phthalocyanine

Guidance literature:: In neat (no solvent); 0.9 mmol of dinitrile and 0.25 mmol of metal chloride heated in a quartz ampoule at 190-195°C for 30 min; melt washed with dilute HCl until colorless filtrate and then with H2O;dried at 60°C; extd. with CHCl3, solvent removed in vacuo; residue chromd. on alumina column with CHCl3-alcohol (2:1) as eluent; identified by elem. anal.;

Reference yield: 18.0%

: copper dichloride

: 329326-24-1
5-nitro-4-[4-(phenylazo)phenoxy]phthalodinitrile

: 329246-17-5
copper tetra-5-nitrotetra-4-((4-phenylazo)phenoxy)phthalocyanine

Guidance literature:: In neat (no solvent); 0.9 mmol of dinitrile and 0.25 mmol of metal chloride heated in a quartz ampoule at 190-195°C for 30 min; melt washed with dilute HCl until colorless filtrate and then with H2O;dried at 60°C; extd. with CHCl3, solvent removed in vacuo; residue chromd. on alumina column with CHCl3-alcohol (2:1) as eluent; identified by elem. anal.;