1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane

Base Information

• Chemical Name: 1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane
• CAS No.: 1380511-71-6
• Molecular Formula: C₇₂H₁₄OS₂
• Molecular Weight: 959.035

Synonyms:1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane

Chemical Property of 1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane

Chemical Property:

Purity/Quality:

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Technology Process of 1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane

There total 1 articles about 1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C₆₀-Ih)[5,6]fullero[2',3':1,9]cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

C12H14N2OS2 (1380511-68-1) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 1'-[2''-(methylthio)ethyl]-1'-[S-benzylcarbothioyl]-(C60-Ih)[5,6]fullero[2',3':1,9]cyclopropane (1380511-71-6)

Guidance literature:

With bis(acetylacetonato)palladium(II); triethylaluminum; triphenylphosphine; In 1,2-dichloro-benzene; toluene; at 40 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.04.017

upstream raw materials:

C₁₂H₁₄N₂OS₂

fullerene-C₆₀

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