Technology Process of 1-oxo-1H-indene-5-carboxylic acid trityl-amide
There total 4 articles about 1-oxo-1H-indene-5-carboxylic acid trityl-amide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
tetrachloromethane;
for 2h;
Heating;
DOI:10.1021/jm9903242
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 5 percent / 3percent aq. H2O2 / 4 h / 50 °C
2: 44 percent / acetic anhydride; conc. aq. H2SO4 / acetic acid / 3.5 h / 40 °C
3: 47 percent / N-bromosuccinimide / CCl4 / 2 h / Heating
With
N-Bromosuccinimide; sulfuric acid; acetic anhydride;
In
tetrachloromethane; acetic acid;
1: Oxidation / 2: Condensation / 3: Dehydration;
DOI:10.1021/jm9903242
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / tetrakis(triphenylphosphine) palladium(O) / dimethylformamide / 2 h / 80 °C
2: 5 percent / 3percent aq. H2O2 / 4 h / 50 °C
3: 44 percent / acetic anhydride; conc. aq. H2SO4 / acetic acid / 3.5 h / 40 °C
4: 47 percent / N-bromosuccinimide / CCl4 / 2 h / Heating
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sulfuric acid; acetic anhydride;
In
tetrachloromethane; acetic acid; N,N-dimethyl-formamide;
1: Substitution / 2: Oxidation / 3: Condensation / 4: Dehydration;
DOI:10.1021/jm9903242
