3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

Base Information

Chemical Name:3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester
CAS No.:1032611-25-8
Molecular Formula:C₂₅H₂₇IO₈
Molecular Weight:582.389
Hs Code.:

Synonyms:3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

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Chemical Property of 3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

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Technology Process of 3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

There total 1 articles about 3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1032611-21-4
3-(2-iodo-3-methoxyphenyl)-3-oxopropionic acid methyl ester

: 1032611-24-7
3-allyl-4-bromomethyl-2,6-dimethoxybenzoic acid methyl ester

: 1032611-25-8
3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

Guidance literature:: 3-(2-iodo-3-methoxyphenyl)-3-oxopropionic acid methyl ester; With sodium methylate; In methanol; at 20 ℃; for 1h;

3-allyl-4-bromomethyl-2,6-dimethoxybenzoic acid methyl ester; With sodium iodide; In methanol; at 130 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1002/chem.200701676

Reference yield: 61.0%

: 25260-60-0
cis-1,4-bis(acetyloxy)but-2-ene

: 1032611-25-8
3-allyl-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

: 3-(4-acetoxybut-2-enyl)-4-[3-(2-iodo-3-methoxyphenyl)-2-methoxycarbonyl-3-oxopropyl]-2,6-dimethoxybenzoic acid methyl ester

Guidance literature:: With (1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)(PCy₃)Cl₂Ru=CHPh; In dichloromethane; at 50 ℃; for 25h;
DOI:10.1002/chem.200701676