2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

Base Information

Chemical Name:2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride
CAS No.:1412906-23-0
Molecular Formula:C₁₃H₁₃F₃N₂O₂*ClH
Molecular Weight:322.715
Hs Code.:

Synonyms:2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

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Chemical Property of 2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

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Technology Process of 2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

There total 5 articles about 2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1412906-22-9
4-oxo-5-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrole-2-carboxylic acid tert-butyl ester

: 1412906-23-0
2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate;

Reference yield:

: 5-benzyl-2-(4-trifluoromethoxy-phenyl)-tetrahydro-pyrrolo[3,4-c]pyrrole-1,3-dione

: 1412906-23-0
2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane; ethanol / 2 h / -40 - -35 °C

2: trifluoroacetic acid; sodium cyanoborohydride / 20 °C

3: hydrogen / palladium on activated charcoal / methanol / 20 °C

4: hydrogenchloride / ethyl acetate

With hydrogenchloride; sodium tetrahydroborate; cerium(III) chloride heptahydrate; hydrogen; sodium cyanoborohydride; trifluoroacetic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 68255-58-3
1-(4-(trifluoromethoxy)phenyl)-1H-pyrrole-2,5-dione

: 1412906-23-0
2-(4-trifluoromethoxy-phenyl)-hexahydro-pyrrolo[3,4-c]pyrrol-1-one, hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane; ethanol / 2 h / -40 - -35 °C

3: trifluoroacetic acid; sodium cyanoborohydride / 20 °C

4: hydrogen / palladium on activated charcoal / methanol / 20 °C

5: hydrogenchloride / ethyl acetate

With hydrogenchloride; sodium tetrahydroborate; cerium(III) chloride heptahydrate; hydrogen; sodium cyanoborohydride; trifluoroacetic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; ethyl acetate;