2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

Base Information

Chemical Name:2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide
CAS No.:1443108-35-7
Molecular Formula:C₁₈H₁₄Br₂N₄O₃
Molecular Weight:494.142
Hs Code.:

Synonyms:2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

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Chemical Property of 2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

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Technology Process of 2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

There total 3 articles about 2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3281-09-2
2-(5,7-dibromoquinolin-8-yloxy)acetohydrazide

: 103-71-9
phenyl isocyanate

: 1443108-35-7
2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

Guidance literature:: In ethanol; for 9h; Reflux;
DOI:10.1016/j.ejmech.2013.03.008

Reference yield:

: 521-74-4
broxyquinoline

: 1443108-35-7
2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / Reflux

2: acetic acid; hydrazine hydrate / ethanol / 3 h / 20 °C

3: ethanol / 9 h / Reflux

With potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.03.008

Reference yield:

: 131924-26-0
ethyl 2-(5,7-dibromoquinolin-8-yloxy)acetate

: 1443108-35-7
2-(2-(5,7-dibromoquinolin-8-yloxy)acetyl)-N-phenylhydrazinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; hydrazine hydrate / ethanol / 3 h / 20 °C

2: ethanol / 9 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2013.03.008