C₁₂H₁₂⁽²⁾HNO₄

Base Information

Chemical Name:C₁₂H₁₂⁽²⁾HNO₄
CAS No.:139732-03-9
Molecular Formula:C₁₂H₁₃NO₄
Molecular Weight:236.232
Hs Code.:

C<sub>12</sub>H<sub>12</sub><sup>(2)</sup>HNO<sub>4</sub>

Synonyms:C₁₂H₁₂⁽²⁾HNO₄

Suppliers and Price of C₁₂H₁₂⁽²⁾HNO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂⁽²⁾HNO₄

Chemical Property:

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Technology Process of C₁₂H₁₂⁽²⁾HNO₄

There total 4 articles about C₁₂H₁₂⁽²⁾HNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 139758-43-3
C₁₁H₁₄⁽²⁾HNO₃

: 139731-95-6
C₁₂H₁₂⁽²⁾HNO₄

: 139732-03-9
C₁₂H₁₂⁽²⁾HNO₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 16h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00034a035

Reference yield:

: 139732-01-7
C₁₄H₁₈⁽²⁾HNO₃

: 139732-03-9
C₁₂H₁₂⁽²⁾HNO₄

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 0.2 N aq. HCl / methanol / 0.5 h / Ambient temperature

2: diisopropylethylamine / CH₂Cl₂ / 16 h / 0 - 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/ja00034a035

Reference yield:

: 139731-96-7
methyl (4(S)-phenyloxazolidin-2-on-3-yl)acetate

: 139731-95-6
C₁₂H₁₂⁽²⁾HNO₄

: 139732-03-9
C₁₂H₁₂⁽²⁾HNO₄

Guidance literature:: With deuteromethanol; tert.-butyl lithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -78 deg C, 2.) THF, a) -78 deg C, 15 min, b) -20 deg C, 10 min;
DOI:10.1021/ja00034a035