C₁₅H₁₈O₄

Base Information

Chemical Name:C₁₅H₁₈O₄
CAS No.:1622095-33-3
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:

C<sub>15</sub>H<sub>18</sub>O<sub>4</sub>

Synonyms:C₁₅H₁₈O₄

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Chemical Property of C₁₅H₁₈O₄

Chemical Property:

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Technology Process of C₁₅H₁₈O₄

There total 9 articles about C₁₅H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1622095-26-4
C₁₅H₂₀O₄

: 1622095-33-3
C₁₅H₁₈O₄

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 40h;
DOI:10.1002/ejoc.201402096

Reference yield:

: 99865-70-0
4-(4-Formyl-phenoxy)butyric acid

: 1622095-33-3
C₁₅H₁₈O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C

2.1: dichloromethane / 14 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

3.2: 11.5 h / -78 - -5 °C

4.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / Cooling with ice

5.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

6.1: diazomethyl-trimethyl-silane / diethyl ether; hexane / 0.33 h / Cooling with ice

7.1: manganese(IV) oxide / dichloromethane / 40 h / 20 °C

With dmap; manganese(IV) oxide; lithium hydroxide monohydrate; dihydrogen peroxide; sodium hexamethyldisilazane; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diazomethyl-trimethyl-silane; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; water; 2.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-18-4
C₂₄H₂₅NO₆

: 1622095-33-3
C₁₅H₁₈O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

1.2: 11.5 h / -78 - -5 °C

2.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 1.5 h / Cooling with ice

3.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

4.1: diazomethyl-trimethyl-silane / diethyl ether; hexane / 0.33 h / Cooling with ice

5.1: manganese(IV) oxide / dichloromethane / 40 h / 20 °C

With manganese(IV) oxide; lithium hydroxide monohydrate; dihydrogen peroxide; sodium hexamethyldisilazane; diisobutylaluminium hydride; diazomethyl-trimethyl-silane; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; water;
DOI:10.1002/ejoc.201402096