3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

Base Information

Chemical Name:3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate
CAS No.:360771-94-4
Molecular Formula:C₂₉H₃₂O₆
Molecular Weight:476.569
Hs Code.:

3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5<sup>(10)</sup>-estratrien-6-one acetate

Synonyms:3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

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Technology Process of 3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

There total 5 articles about 3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-24-7
acetic anhydride

: 360771-93-3
3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one

: 360771-94-4
3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

Guidance literature:: With pyridine;
DOI:10.1016/S0039-128X(00)00236-1

Reference yield:

: 100-44-7
benzyl chloride

: 360771-94-4
3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / K₂CO₃ / ethanol / 7 h / Heating

2: 95 percent / pyridine

With pyridine; potassium carbonate; In ethanol;
DOI:10.1016/S0039-128X(00)00236-1

Reference yield:

: 360771-92-2
3,4-dihydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one

: 360771-94-4
3-benzyloxy-4-hydroxy-17,17-ethylenedioxy-1,3,5⁽¹⁰⁾-estratrien-6-one acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / K₂CO₃ / ethanol / 7 h / Heating

2: 95 percent / pyridine

With pyridine; potassium carbonate; In ethanol;
DOI:10.1016/S0039-128X(00)00236-1