3-chloro-4-nitrobenzenethiol

Base Information

Chemical Name:3-chloro-4-nitrobenzenethiol
CAS No.:119982-64-8
Molecular Formula:C₆H₄ClNO₂S
Molecular Weight:189.622
Hs Code.:

Synonyms:3-chloro-4-nitrobenzenethiol

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Chemical Property of 3-chloro-4-nitrobenzenethiol

Chemical Property:

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Technology Process of 3-chloro-4-nitrobenzenethiol

There total 1 articles about 3-chloro-4-nitrobenzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 14371-79-0
2-nitro-5-chlorothiophenol

: 119982-64-8
3-chloro-4-nitrobenzenethiol

Guidance literature:: With sodium sulfide; In methanol; at 20 ℃; for 23h;
DOI:10.1002/jhet.5570380520

Reference yield: 80.0%

: 119982-64-8
3-chloro-4-nitrobenzenethiol

: 105905-34-8
2-chloro-4-[(3-chloro-4-nitrophenyl)disulfanyl]-1-nitrobenzene

Guidance literature:: With sodium hydrogensulfite; periodic acid; In water; at 20 ℃; for 1.56667h;
DOI:10.2174/157017810791514733

Reference yield:

: 119982-64-8
3-chloro-4-nitrobenzenethiol

: 60854-81-1
2-chloro-4-(methylsulfonyl)-1-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 0-5 deg C, 1 h, 2.) DMF, 5 deg C, 1 h

2: 79 percent / 30percent aq. H₂O₂ / acetic acid / 2 h / 80 °C

With dihydrogen peroxide; sodium hydride; In acetic acid;
DOI:10.1248/cpb.41.894