3-methoxy-2-nitrobenzoyl azide

Base Information

• Chemical Name: 3-methoxy-2-nitrobenzoyl azide
• CAS No.: 90321-73-6
• Molecular Formula: C₈H₆N₄O₄
• Molecular Weight: 222.16
• Mol file: 90321-73-6.mol

Synonyms:3-methoxy-2-nitrobenzoyl azide

Chemical Property of 3-methoxy-2-nitrobenzoyl azide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methoxy-2-nitrobenzoyl azide

There total 3 articles about 3-methoxy-2-nitrobenzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-3-methoxybenzoyl chloride (15865-57-3) → 3-methoxy-2-nitrobenzoyl azide (90321-73-6)

Guidance literature:

With sodium azide; In water; acetone; for 0.5h; Ambient temperature;

DOI:10.1021/jm00063a013

Reference yield:

3-methoxy-2-nitrobenzoic acid (4920-80-3) → 3-methoxy-2-nitrobenzoyl azide (90321-73-6)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride, DMF / toluene / 0.5 h / Heating

2: aq. NaN₃ / acetone / 1 h

With thionyl chloride; sodium azide; N,N-dimethyl-formamide; In acetone; toluene;

DOI:10.1021/jm960442e

Reference yield:

→ 3-methoxy-2-nitrobenzoyl azide (90321-73-6)

Guidance literature:

2-Nitro-3-methoxy-benzoesaeure-hydrazid in Dioxan + DMF + 6n-HCl u. NaNO2-Lsg.;

upstream raw materials:

2-nitro-3-methoxybenzoyl chloride

3-methoxy-2-nitrobenzoic acid

Downstream raw materials:

3-methoxy-2-nitroaniline

(2-Benzylamino-3-methoxy-phenyl)-carbamic acid tert-butyl ester

1-Benzyl-2-chloro-7-methoxy-1H-benzoimidazole

1-Benzyl-7-methoxy-1,3-dihydro-benzoimidazol-2-one