C₁₄H₁₄INO

Base Information

• Chemical Name: C₁₄H₁₄INO
• CAS No.: 1486476-90-7
• Molecular Formula: C₁₄H₁₄INO
• Molecular Weight: 339.176
• Mol file: 1486476-90-7.mol

Synonyms:C₁₄H₁₄INO

Chemical Property of C₁₄H₁₄INO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₄H₁₄INO

There total 1 articles about C₁₄H₁₄INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

styrene oxide (96-09-3) + 2-iodophenylamine (615-43-0) → C14H14INO (1486476-90-7)

Guidance literature:

With 20% cobalt ferrite and reduced graphene oxide nanohybrids; In neat (no solvent); at 80 ℃; for 0.25h; Reagent/catalyst;

DOI:10.1016/j.molstruc.2019.127522

Reference yield: 84.0%

2-Phenyl-3-butyn-2-ol (127-66-2) + C14H14INO (1486476-90-7) → C24H23NO2

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 50 ℃; Inert atmosphere;

DOI:10.1002/asia.201201249

Reference yield:

C14H14INO (1486476-90-7) → C24H21NO

Guidance literature:

Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 50 °C / Inert atmosphere

2: (1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene)gold(I) chloride; silver(I) triflimide / toluene / 3.5 h / 50 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; (1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene)gold(I) chloride; triethylamine; silver(I) triflimide; In toluene; 1: |Sonogashira Cross-Coupling;

DOI:10.1002/asia.201201249

upstream raw materials:

styrene oxide

2-iodophenylamine